32
may be measured relative to a control sample. The transmission of each sample
was measured relative to air.
Figure 4-10: Photograph of the Varian Cary 500 spectrophotometer.
Samples were tested prior to irradiation as well as on the day of irradiation, 1
day, 2 days, 1 week and 4 weeks after irradiation. Testing was done over several
days after irradiation in order to observe healing of the transpare ncy loss in the
scintillators. Measurements were also made for a control sample for each grade
on each respective day in order to correct for any day to day systematic
fluctuations.
A baseline as well as zeroing calibration were performed on the machine p rior to
each days testing. Measurements were taken for four different mounting positions
of the sample within the machine (2 per cross-sectional face) and the average
spectra was processed for analysis thereafter. Samples were mounted behind a
slide containing a 1 mm diameter hole through which light was incident, thereby
ensuring that only the irradiated regio ns of each sample was measured.
4.2.2.
Light yield testing in response to
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