SPbOPEN 2019
Journal of Physics:
Conference Series
1410 (2019) 012230
IOP Publishing
doi:10.1088/1742-6596/1410/1/012230
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pressure of 3 to 5 ∙ 10
-5
Pa to eliminate the reaction gas gettering which manifests itself during
magnetron sputtering as a result of plasma radiation.
When ion-beam sputtering, the target and the
substrate are outside the plasma, which qualitatively improves the structure properties [13].
The substrate temperature was varied from 150 to 350 °C. Textures with
satisfactory properties are
formed at 350 °C. The pressure of the working mixture in the vacuum chamber was maintained in the
range from 1 to 3 ∙ 10
-3
Pa in the ratio of gases Ar : N2 = 1 : 1. When reducing the argon percentage, a
decrease in the rate of the target material sputtering and the deterioration of the deposited film
properties are observed. This is due to the chemical activity of nitrogen entering into the compound
with the target
material on its surface, and the insufficient energy of the bombarding ions compared
with the kinetic energy of argon ions for intensive ejection of atoms and atoms conglomerates
(clusters) from the target [13].
The disadvantages of the ion-beam method of sputtering AlN include the relatively low reproducibility
of the resulting films properties and the structures defectiveness due to knocking out clusters (atoms
conglomerates) that degrade the film texture.
ZnO thin films with piezoelectric properties were obtained by reactive HF-magnetron target sputtering
from Zn (99.9 %) in an Ar + 65% O
2
gas mixture at a chamber pressure of 1 to 3 ∙ 10
-3
Pa. The
substrate temperature was 220 °C, the RF discharge power was 100 W. The use of RF magnetron
target sputtering from Zn (99.9 %) instead of DC sputtering is caused by the “poisoning” of the target
with oxygen and the formation of a surface dielectric layer contributing to the appearance of a surface
charge reducing the sputtering rate. In addition, when HF target sputtering ZnO, it often cracks as a
result of overheating. The exclusion of thermo-mechanical stresses was
carried out by carrying out
heating and cooling in both cases at a rate of not more than 3 °C/min. Sputtering of piezoelectric
structures in combination with the spent silicon technology for obtaining strain gages can be carried
out both before the formation of strain gages and after.
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